Development of Armillae mellea immobilized nanodiamond for the preconcentrations of Cr(III), Hg(II) and Zn(II)

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dc.contributor.authorKılınç, Ersin
dc.contributor.authorOzdemir, Sadin
dc.contributor.authorŞen, Fatih
dc.contributor.authorSoylak, Mustafa
dc.date.accessioned2021-07-19T07:27:39Z
dc.date.available2021-07-19T07:27:39Z
dc.date.issued2021en_US
dc.departmentMAÜ, Meslek Yüksekokulları, Sağlık Hizmetleri Meslek Yüksekokulu, Tıbbi Hizmetler ve Teknikler Bölümüen_US
dc.description.abstractIn this study, we present an environmental friend and easy procedure for simultaneous preconcentration of Cr(III), Hg(II) and Zn(II) by solid-phase extraction before their determination by inductively coupled plasma optical emission spectrometry. Armillae mellea immobilized nanodiamond was used as sorbent. During the study, critical parameters influencing the extraction performance were investigated in detail. The best parameters were found as pH 5.0, 2.0 mL min−1 of flow rate, 200 mg of Armillae mellea, 300 mL of sample volume. LOD values were found as 0.025, 0.13 and 0.038 ng mL−1, respectively for Cr(III), Hg(II) and Zn(II). By applying the developed procedure, sensitivities of ICP-OES were improved for 60 fold for Cr(III), Hg(II) and Zn(II). Their concentrations in different food samples were measured after microwave digestion and solid-phase extraction.en_US
dc.identifier.citationOzdemir S, Kılınç E, Şen F, Soylak M. Development of Armillae mellea immobilized nanodiamond for the preconcentrations of Cr(III), Hg(II) and Zn(II). Anal Biochem. 2021 Mar 15;617:114122. doi: 10.1016/j.ab.2021.114122. Epub 2021 Jan 28. PMID: 33515499.
dc.identifier.doi10.1016/j.ab.2021.114122en_US
dc.identifier.pmid33515499en_US
dc.identifier.scopus2-s2.0-85100423571en_US
dc.identifier.scopusqualityN/Aen_US
dc.identifier.urihttps://www.scopus.com/record/display.uri?eid=2-s2.0-85100423571&doi=10.1016%2fj.ab.2021.114122&origin=inward&txGid=5c514ba1e305920aaceaeccb08fc41ed&featureToggles=FEATURE_NEW_METRICS_SECTION:1
dc.identifier.urihttps://hdl.handle.net/20.500.12514/2685
dc.identifier.volume617en_US
dc.identifier.wosWOS:000620422800002en_US
dc.identifier.wosqualityQ3en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.indekslendigikaynakPubMeden_US
dc.language.isoenen_US
dc.publisherAnalytical Biochemistryen_US
dc.relation.ispartofAnalytical Biochemistryen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectFood analysis, Metal ions, Preconcentration, Sensitivity enhancement, Solid-phase extractionen_US
dc.titleDevelopment of Armillae mellea immobilized nanodiamond for the preconcentrations of Cr(III), Hg(II) and Zn(II)en_US
dc.typeArticleen_US

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