Fabrication and characterization of Fe3O4/perlite, Fe3O4/perlite@SiO2, and Fe3O4/perlite@SiO2@sulfanilamide magnetic nanomaterials

Basit Öğe Kaydı
dc.contributor.authorKutluay, Sinan
dc.contributor.authorŞahin, Ömer
dc.contributor.authorEce, Mehmet Şakir
dc.date.accessioned2022-05-13T08:08:08Z
dc.date.available2022-05-13T08:08:08Z
dc.date.issued2022en_US
dc.departmentMAÜ, Meslek Yüksekokulları, Sağlık Hizmetleri Meslek Yüksekokulu, Tıbbi Hizmetler ve Teknikler Bölümüen_US
dc.description.abstractAbstract In this study, the fabrication of perlite-supported Fe3O4 (Fe3O4/perlite), SiO2-coated Fe3O4/perlite (Fe3O4/perlite@SiO2), and sulfanilamide-modified Fe3O4/perlite@SiO2 (Fe3O4/perlite@SiO2@sulfanilamide) magnetic nanomaterials and their characterization by various spectroscopic techniques were presented. For this purpose, first, Fe3O4/perlite was fabricated via the co-precipitation method. Then, Fe3O4/perlite@SiO2 and Fe3O4/perlite@SiO2@sulfanilamide nanomaterials were fabricated using the sol–gel method. The structural properties of the fabricated nanomaterials were characterized using Brunauer-Emmett-Teller (BET), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), SEM-energy-dispersive X-ray spectroscopy (EDX), thermogravimetric analysis-differential thermal analysis, and X-ray diffraction (XRD) analyses. The SEM, SEM–EDX, FTIR, and XRD analyses revealed that the fabrication and surface coatings of the Fe3O4/perlite, Fe3O4/perlite@SiO2, and Fe3O4/perlite@SiO2@sulfanilamide were successfully performed. It was concluded that the Fe3O4/perlite, Fe3O4/perlite@SiO2, and Fe3O4/perlite@SiO2@sulfanilamide showed a type IV-H3 hysteresis loop according to the International Union of Pure and Applied Chemistry classification. According to the BET analysis, it was found that the specific surface areas of the Fe3O4/perlite, Fe3O4/perlite@SiO2, and Fe3O4/perlite@SiO2@sulfanilamide were 8.09, 12.71, and 5.89 m2/g, respectively. The average pore radius of the Fe3O4/perlite, Fe3O4/perlite@SiO2, and Fe3O4/perlite@SiO2@sulfanilamide were 9.68, 7.91, and 34.69 nm, respectively, using the Barrett-Joyner-Halenda method. Moreover, the half-pore widths of the Fe3O4/perlite, Fe3O4/perlite@SiO2, and Fe3O4/perlite@SiO2@sulfanilamide were 2.27, 1.58, and 17.99 nm, respectively, using the density functional theory method. Furthermore, in light of characterization findings, the Fe3O4/perlite, Fe3O4/perlite@SiO2, and Fe3O4/perlite@SiO2@sulfanilamide were in crystalline cubic spinel form, and they had mechanical and thermal stability and a mesoporous structure. Within the framework of the results, these developed nanomaterials, which have potential in many applications, such as sustainable technologies and environmental safety technologies, were brought to the attention of related fields.en_US
dc.identifier.citationKutluay, S., Şahin, Ö., & Ece, M. Ş. (2022). Fabrication and characterization of Fe3O4/perlite, Fe3O4/perlite@ SiO2, and Fe3O4/perlite@ SiO2@ sulfanilamide magnetic nanomaterials. Applied Physics A, 128(3), 1-14.en_US
dc.identifier.doi10.1007/s00339-022-05369-4en_US
dc.identifier.endpage14en_US
dc.identifier.issue3en_US
dc.identifier.scopus2-s2.0-85125463794en_US
dc.identifier.scopusqualityN/Aen_US
dc.identifier.startpage1en_US
dc.identifier.urihttps://doi.org/10.1007/s00339-022-05369-4
dc.identifier.urihttps://www.scopus.com/record/display.uri?eid=2-s2.0-85125463794&origin=SingleRecordEmailAlert&dgcid=raven_sc_affil_en_us_email&txGid=dcaf55b1d1f48b3dd2fcbb2f3ccdd9ef&featureToggles=FEATURE_NEW_DOC_DETAILS_EXPORT:1
dc.identifier.urihttps://hdl.handle.net/20.500.12514/3103
dc.identifier.urihttps://www.webofscience.com/wos/woscc/full-record/WOS:000758821000004?AlertId=d383397b-4355-449e-9419-70f9e0e77c15&SID=EUW1ED0B7DlgpOiiOdSHvSwg1rjbA
dc.identifier.volume128en_US
dc.identifier.wosWOS:000758821000004en_US
dc.identifier.wosqualityQ2en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherSpringerLinken_US
dc.relation.ispartofApplied Physics Aen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectCharacterization; Fe3O4/perlite; Fe3O4/perlite@SiO2; Fe3O4/perlite@SiO2@sulfanilamide; Magnetic nanomaterials; Nanotechnologyen_US
dc.titleFabrication and characterization of Fe3O4/perlite, Fe3O4/perlite@SiO2, and Fe3O4/perlite@SiO2@sulfanilamide magnetic nanomaterialsen_US
dc.typeArticleen_US

Dosyalar

Orijinal paket
Listeleniyor 1 - 1 / 1
Küçük Resim Yok
İsim:
Kutluay2022_Article_FabricationAndCharacterization.pdf
Boyut:
4.81 MB
Biçim:
Adobe Portable Document Format
Açıklama:
Full Text - Article
İndir
Lisans paketi
Listeleniyor 1 - 1 / 1
Küçük Resim Yok
İsim:
license.txt
Boyut:
1.44 KB
Biçim:
Item-specific license agreed upon to submission
Açıklama:
İndir

Koleksiyon

Scopus İndeksli Yayınlar Koleksiyonu
Tıbbi Hizmetler ve Teknikler Bölümü Koleksiyonu
WoS İndeksli Yayınlar Koleksiyonu