Preconcentration of Sn in Real Water Samples by Solid Phase Extraction Based on the Use of Helvella leucopus as a Fungal Biomass Prior to its Determination by ICP-OES

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dc.contributor.authorKilinc, Ersin
dc.contributor.authorDundar, Abdurrahman
dc.contributor.authorOzdemir, Sadin
dc.contributor.authorOkumus, Veysi
dc.date.accessioned2021-09-22T12:12:50Z
dc.date.available2021-09-22T12:12:50Z
dc.date.issued2013en_US
dc.departmentMAÜ, Meslek Yüksekokulları, Sağlık Hizmetleri Meslek Yüksekokulu, Tıbbi Hizmetler ve Teknikler Bölümüen_US
dc.description.abstractRecently, biosorbents of biological origin such as fungus, algae, and bacteria have found special application as packing material in solid phase extraction (SPE). In this study, an alternative SPE method was developed and validated for the preconcentration of Sn prior to its determination by inductively coupled plasma optical emission spectrometry (ICP-OES). Helvella leucopus, a fungal biomass, was used as the biosorbent in the column studies. Experimental parameters, such as pH and flow rate of the solution, amounts of biosorbent and resin, and volume of the sample solution which affects the analytical results, were investigated. Effects of possible interfering ions on the SPE preconcentration of Sn were investigated. The sensitivity of ICP-OES was improved 47.1 times for Sn. The LOD and LOQ values were 0.06 and 0.21 ng respectively. Linearity was obtained in the concentration range of 1.0-30 ng mL(-1) for Sn. The loading capacity of Helvella leucopus immobilized Amberlite XAD-4 was 10.4 mg g(-1). The concentrations of Sn in the water samples from the Tigris River were determined using the developed method and validated by analysis of the certified reference material NWTM-26.3 Fortified Water sample.en_US
dc.identifier.citationKılınç, E. (2013). Preconcentration of Sn in Real Water Samples by Solid Phase Extraction Based on the Use of Helvella leucopus as a Fungal Biomass Prior to its Determination by ICP-OES. Atomic Spectroscopy, 34(4), 133–139. https://doi.org/10.46770/as.2013.04.004en_US
dc.identifier.doi10.46770/AS.2013.04.004en_US
dc.identifier.endpage139en_US
dc.identifier.issue4en_US
dc.identifier.scopus2-s2.0-84884791489en_US
dc.identifier.scopusqualityN/Aen_US
dc.identifier.startpage133en_US
dc.identifier.uri0195-5373
dc.identifier.urihttps://hdl.handle.net/20.500.12514/2863
dc.identifier.volume34en_US
dc.identifier.wosWOS:000324842200004en_US
dc.identifier.wosqualityQ2en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherATOMIC SPECTROSCOPYen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.subjectCLOUD POINT EXTRACTION;FOOD SAMPLES;SILICA-GEL;TIN;SPECTROMETRY;SPECIATION;SN(IV);RESIN;LEAD;BIOSORPTIONen_US
dc.titlePreconcentration of Sn in Real Water Samples by Solid Phase Extraction Based on the Use of Helvella leucopus as a Fungal Biomass Prior to its Determination by ICP-OESen_US
dc.typeArticleen_US

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