Anoxybacillus sp. SO B1-Immobilized Amberlite XAD-16 for Solid-Phase Preconcentration of Cu(II) and Pb(II) and Their Determinations by Flame Atomic Absorption Spectrometry

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dc.contributor.authorOral, Elif Varhan
dc.contributor.authorOzdemir, Sadin
dc.contributor.authorDolak, Ibrahim
dc.contributor.authorOkumus, Veysi
dc.contributor.authorDundar, Abdurrahman
dc.contributor.authorZiyadanogullari, Berrin
dc.contributor.authorAksoy, Zehra
dc.contributor.authorOnat, Ruken
dc.date.accessioned14.07.201910:50:10
dc.date.accessioned2019-07-16T20:44:04Z
dc.date.available14.07.201910:50:10
dc.date.available2019-07-16T20:44:04Z
dc.date.issued2015
dc.departmentMAÜ, Meslek Yüksekokulları, Sağlık Hizmetleri Meslek Yüksekokulu, Tıbbi Hizmetler ve Teknikler Bölümüen_US
dc.description.abstractA new method for the determination of Cu(II) and Pb(II) by flame atomic absorption spectrometry (FAAS) after preconcentrating on a column containing Anoxybacillus sp. SO B1-immobilized Amberlite XAD-16 was developed. The functional groups of Anoxybacillus sp. SO B1 immobilized on Amberlite XAD-16 were characterized in KBr tablets by Fourier transform infrared (FT-IR) spectrometry. Various parameters such as pH, amount of the adsorbent, eluent type and volume, and flow rate of the sample solution were studied. The optimum pH values of quantitative sorption for Cu(II) and Pb(II) were found to be pH 7.0 and 5.0 and Cu(II) and Pb(II) ions could be quantitatively eluted with 5.0ml of 1.0mol L-1 HCI and 10.0ml of 0.25mol L-1 HNO3, respectively. Recoveries of Cu(II) and Pb(II) were found to be 100.9 +/- 1.57% and 100.3 +/- 0.49% (N = 5), the limits of detection of Cu(II) and Pb(II) in the determination by FAAS (3s, N = 10) were found to be 0.8 and 1.6 mu g L-1, respectively. The proposed enrichment method was applied for metal ion determination from water samples such as two parts of Tigris River water in Diyarbakir and Elazig, Lake of Hazar in Elazig, and tap water in Diyarbakir. Furthermore, the accuracy of the proposed method was verified by studying the analytical recovery and by analyzing certified reference material (NCS-DC 73350 leaves of poplar).en_US
dc.identifier.citationOral, E. V., Ozdemir, S., Dolak, I., Okumus, V., Dundar, A., Ziyadanogullari, B., Aksoy, Z., & Onat, R. (2015). Anoxybacillussp. SO B1–Immobilized Amberlite XAD-16 for Solid-Phase Preconcentration of Cu(II) and Pb(II) and Their Determinations by Flame Atomic Absorption Spectrometry. Bioremediation Journal, 19(2), 139–150. https://doi.org/10.1080/10889868.2014.978837
dc.identifier.doi10.1080/10889868.2014.978837en_US
dc.identifier.endpage150en_US
dc.identifier.issn1088-9868
dc.identifier.issn1547-6529
dc.identifier.issue2en_US
dc.identifier.scopus2-s2.0-84930243624en_US
dc.identifier.scopusqualityQ2en_US
dc.identifier.startpage139en_US
dc.identifier.urihttps://dx.doi.org/10.1080/10889868.2014.978837
dc.identifier.urihttps://hdl.handle.net/20.500.12514/1373
dc.identifier.volume19en_US
dc.identifier.wosWOS:000355261100005en_US
dc.identifier.wosqualityQ4en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherTAYLOR & FRANCIS INCen_US
dc.relation.ispartofBIOREMEDIATION JOURNALen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectenrichment methoden_US
dc.subjectimmobilizationen_US
dc.subjectamberlite XAD-16en_US
dc.subjectflame atomic absorption spectrometryen_US
dc.subjectAnoxybacillus sp. SO B1en_US
dc.titleAnoxybacillus sp. SO B1-Immobilized Amberlite XAD-16 for Solid-Phase Preconcentration of Cu(II) and Pb(II) and Their Determinations by Flame Atomic Absorption Spectrometryen_US
dc.typeArticleen_US

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