Synthesis and characterization of activated carbon supported magnetic nanoparticles (Fe3O4/AC@SiO2@Sulfanilamide) and its application in removal of toluene and benzene

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dc.contributor.authorEce, Mehmet Şakir
dc.date.accessioned2021-07-14T08:27:08Z
dc.date.available2021-07-14T08:27:08Z
dc.date.issued2021en_US
dc.departmentMAÜ, Meslek Yüksekokulları, Sağlık Hizmetleri Meslek Yüksekokulu, Tıbbi Hizmetler ve Teknikler Bölümüen_US
dc.description.abstractIn this study, the Fe3O4/AC@SiO2@Sulfanilamide magnetic nanoparticles were successfully synthesized as a highly effective magnetic nano adsorbent and applied for the adsorption of toluene and benzene in the gas phase for the first time. The magnetic nano-adsorbents were characterized by the Brunauer-Emmett-Teller surface area analysis, Differential Thermal Analysis, Thermal Gravimetric Analysis, Fourier Transform Infrared Spectroscopy, Vibrating Sample Magnetometer, Scanning Electron Microscopy and Energy-Dispersive X-Ray Spectroscopy measurements. Besides, the process parameters that affect the adsorption were optimized using the response surface methodology. Optimum conditions of process factors such as contact time, temperature and initial concentration were determined as 59 min, 25 °C and 18 mg/L for toluene, and as 55 min, 28 °C and 15 mg/L for benzene. The maximum adsorption capacity for toluene and benzene was as 612 and 557 mg/g, respectively, under optimal process conditions. Even after five consecutive repetitions, the Fe3O4/AC@SiO2@Sulfanilamide showed high repeatability and retained 89 % and 88 % of its initial adsorption capacity for toluene and benzene, respectively. Kinetic and equilibrium models were investigated. According to these study results, it can be said that having easy synthesis process, high adsorption capacity and reusability performance makes the Fe3O4/AC@SiO2@Sulfanilamide a promising magnetic nano adsorbent.en_US
dc.description.sponsorshipThis project is funded by the financial support from Mardin Artuklu University (Project No. MAU.BAP.18.SHMYO.030).en_US
dc.identifier.doi10.1016/j.colsurfa.2021.126231en_US
dc.identifier.scopus2-s2.0-85102495231en_US
dc.identifier.scopusqualityN/Aen_US
dc.identifier.urihttps://www.scopus.com/record/display.uri?eid=2-s2.0-85102495231&doi=10.1016%2fj.colsurfa.2021.126231&origin=inward&txGid=c29e1a4ff5a3e8482bbefb8d53a10e45&featureToggles=FEATURE_NEW_METRICS_SECTION:1
dc.identifier.urihttps://hdl.handle.net/20.500.12514/2667
dc.identifier.volume617en_US
dc.identifier.wosWOS:000636785500005en_US
dc.identifier.wosqualityQ2en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherColloids and Surfaces A: Physicochemical and Engineering Aspectsen_US
dc.relation.ispartofColloids and Surfaces A: Physicochemical and Engineering Aspectsen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectActivated carbon supported magnetic nano adsorbents, adsorption/desorption, magnetite/AC/silica/sulfanilamide, Response surface methodology (RSM), Surface coatingen_US
dc.titleSynthesis and characterization of activated carbon supported magnetic nanoparticles (Fe3O4/AC@SiO2@Sulfanilamide) and its application in removal of toluene and benzeneen_US
dc.typeArticleen_US

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