Quantitative determination and removal of pesticide residues in fresh vegetables and fruit products by LC-MS/MS and GC-MS/MS

Basit Öğe Kaydı
dc.contributor.authorElmastas, Ayhan
dc.contributor.authorUmaz, Adil
dc.contributor.authorPirinc, Vedat
dc.contributor.authorAydin, Firat
dc.date.accessioned2023-01-19T05:52:51Z
dc.date.available2023-01-19T05:52:51Z
dc.date.issued2023en_US
dc.departmentMAÜ, Meslek Yüksekokulları, Sağlık Hizmetleri Meslek Yüksekokulu, Tıbbi Hizmetler ve Teknikler Bölümüen_US
dc.description.abstractPesticides are the potent agrochemicals used to successfully manage, repel, or stop pests and weeds in agricultural production. This study analyzed 222 pesticide active substances in 90 samples of seven different vegetables and fruits acquired from producers through liquid chromatography-mass spectrometry/mass spectrometry (LC-MS/MS) and gas chromatography-mass spectrometry/mass spectrometry (GC-MS/MS) technology. The validation parameters of each pesticide's active substances were determined. The LOD, LOQ values, and recovery studies of the 222 active substances were 3.00, 10.00 ng/g, and between 76.07 and 108.08%, respectively. The correlation coefficients and measurement uncertainty were determined to be between 0.990-0.999 and 8.91-31.46%, respectively. There were active substances of chlorpyrifos, acetamiprid, azoxystrobin, difenoconazole, malathion, dieldrin, boscalid, triticonazole, tebuconazole, triadimenol, trifloxystrobin, pirimicarb, and dodine among the vegetable and fruit samples used in the study. There were no active substances in 55 (61%) samples. Among the 35 samples (39%), 31 samples (34%) contained only one active substance, whereas four (5%) contained two active substances. However, the amount of active substances in six (7%) samples was above the maximum residue levels (MRL) limits. Various processes used in the study revealed that peeling was the most effective pesticide residue removal strategy. The washing procedure also proved that it reduced some pesticide residues but failed to eliminate all pesticides. The peeling process successfully reduced a significant amount of the active substances from the products, however, residues remained. Washing the fruits with hot water was also effective in removing residues. As a result, analyses of the peeled sections yielded higher pesticide residue concentrations than those of the entire product.en_US
dc.identifier.citationElmastas, A., Umaz, A., Pirinc, V., & Aydin, F. (2023). Quantitative determination and removal of pesticide residues in fresh vegetables and fruit products by LC–MS/MS and GC–MS/MS. Environmental Monitoring and Assessment, 195(2), 1-32.en_US
dc.identifier.doi10.1007/s10661-022-10910-2en_US
dc.identifier.endpage32en_US
dc.identifier.issue2en_US
dc.identifier.pmid36609771en_US
dc.identifier.scopus2-s2.0-85145773761en_US
dc.identifier.scopusqualityN/Aen_US
dc.identifier.startpage1en_US
dc.identifier.urihttps://doi.org/10.1007/s10661-022-10910-2
dc.identifier.urihttps://pubmed.ncbi.nlm.nih.gov/36609771/
dc.identifier.urihttps://www.scopus.com/record/display.uri?eid=2-s2.0-85145773761&origin=resultslist&sort=plf-f&src=s&st1=10.1007%2fs10661-022-10910-2&sid=95e7f7829d3461a71ba0888c16a6c7ae&sot=b&sdt=b&sl=31&s=DOI%2810.1007%2fs10661-022-10910-2%29&relpos=0&citeCnt=0&searchTerm=
dc.identifier.urihttps://hdl.handle.net/20.500.12514/3346
dc.identifier.volume195en_US
dc.identifier.wosWOS:000910870000002en_US
dc.identifier.wosqualityN/Aen_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.indekslendigikaynakPubMeden_US
dc.language.isoenen_US
dc.publisherSpringerLinken_US
dc.relation.ispartofEnvironmental Monitoring and Assessmenten_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectFruit; GC-MS/MS; LC-MS/MS; Pesticides; Vegetable.en_US
dc.titleQuantitative determination and removal of pesticide residues in fresh vegetables and fruit products by LC-MS/MS and GC-MS/MSen_US
dc.typeArticleen_US

Dosyalar

Orijinal paket
Listeleniyor 1 - 1 / 1
Küçük Resim Yok
İsim:
s10661-022-10910-2.pdf
Boyut:
663.84 KB
Biçim:
Adobe Portable Document Format
Açıklama:
Full Text - Article
İndir
Lisans paketi
Listeleniyor 1 - 1 / 1
Küçük Resim Yok
İsim:
license.txt
Boyut:
1.44 KB
Biçim:
Item-specific license agreed upon to submission
Açıklama:
İndir

Koleksiyon

PubMed İndeksli Yayınlar Koleksiyonu
Scopus İndeksli Yayınlar Koleksiyonu
Tıbbi Hizmetler ve Teknikler Bölümü Koleksiyonu
WoS İndeksli Yayınlar Koleksiyonu